Exothermic dissolution – use a borosilicate beaker in a water bath, PPE, and ventilation. See NaOH safety. Standardise against a primary standard if analytical accuracy is required.
Steps
- Put ~800 ml cold demineralised water in a heat-safe beaker.
- Slowly add 40 g NaOH with stirring; cool as needed.
- Transfer to a 1 L volumetric flask and make up to mark when cool.
- Label with concentration, date, and hazard.
Materials required
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